HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 15671130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 15671128 | HCID 15671128 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15671130 | HCID 15671130 | 55.1% |
Reaction Steps
A procedure similar to that described in Preparation 2 was repeated, except that 5 g of 7-acetoxy-2,8-dimethyl-2-(4-nitrophenoxymethyl)-4-oxochroman (prepared as described in Preparation 17), 980 mg of sodium borohydride and 20 ml of methanol were reacted, to afford 2.77 g of the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873255 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-613ee3793f604ab18001664748dcf9b4 |
| Source note | uspto-grants-1989_10 |