HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15671135, compound → HCID 15671139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15671135 | HCID 15671135 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15671139 | HCID 15671139 | 91.3% |
Reaction Steps
Following a procedure similar to that described in Preparation 4, 1.6 g of 7-acetoxy-2,8-dimethyl-2-(4-nitrophenoxymethyl)-2H-chromene (prepared as described in Preparation 39) was hydrogenated, using 0.2 g of 10% w/w palladium-on-carbon and 15 ml of methanol, to afford 1.35 g of the title compound as a pale brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04873255 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-7f1a5a01788b4011a338e70e79e1b6d7 |
| Source note | uspto-grants-1989_10 |