8(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)- → Indoaniline

HRID 2351551ノート

反応式

HRID 2351551 の反応式
C[C:2]1[CH:7]=[C:6]([N:8](CC)CC)[CH:5]=[CH:4][C:3]=1[N:13]=[C:14]1[CH:23]=[CH:22][C:21](=[O:24])[C:20]2N=CC=C[C:15]1=2>O.C(O)C>[CH:23]1[C:14](=[N:13][C:3]2[CH:2]=[CH:7][C:6]([NH2:8])=[CH:5][CH:4]=2)[CH:15]=[CH:20][C:21](=[O:24])[CH:22]=1

参加物

4

反応物 1

HCID 3648948(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)-

生成物 1

HCID 24748760Indoaniline

試薬・触媒・溶媒 2

HCID 702Ethanol溶媒HCID 962Water溶媒

実験手順

Then, a solution prepared by dissolving 285.3 mg of Ni(ClO4)2.6H2O in 50 ml of water, was added under a nitrogen atmosphere to a solution prepared by dissolving 100 mg of 5-(2'-methyl-4'-diethylaminophenylimino)quinoline-8-one obtained above in 50 ml of 99% ethanol, and the mixture was stirred at room temperature for about 30 minutes. Formed precipitates were subjected to suction filtration, washed with water and dried to obtain a metal-containing indoaniline compound having the formula: ##STR10##

後処理

  1. customThen, a solution prepared
  2. additionwas added under a nitrogen atmosphere to a solution
  3. customprepared
  4. customFormed
  5. customprecipitates
  6. filtrationwere subjected to suction filtration
  7. washwashed with water
  8. customdried

出典と根拠

ORDレコード
ord-7dafeb6eaf2e4289ba34d79329abad9d
出典データセット
uspto-grants-1989_10
特許番号
US04873332

反応ノート

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