8(5H)-Quinolinone, 5-[[4-(diethylamino)-2-methylphenyl]imino]-, (5Z)- → Indoaniline

Participants

Reaction Steps

Then, a solution prepared by dissolving 285.3 mg of Ni(ClO4)2.6H2O in 50 ml of water, was added under a nitrogen atmosphere to a solution prepared by dissolving 100 mg of 5-(2'-methyl-4'-diethylaminophenylimino)quinoline-8-one obtained above in 50 ml of 99% ethanol, and the mixture was stirred at room temperature for about 30 minutes. Formed precipitates were subjected to suction filtration, washed with water and dried to obtain a metal-containing indoaniline compound having the formula: ##STR10##

Provenance & Evidence