Diethyl Ether → HCID 178479226, compound

Participants

Reaction Steps

The compound (I) (0.25 g) was dissolved in a 4N-hydrogen chloride/1,4-dioxane solution (0.76 ml) and the solution was stirred at room temperature for 30 minutes. Diethyl ether (10 ml) was added and the precipitated substance was recovered by filtration. After drying, N-(trans-4-aminomethylcyclohexylcarbonyl)-3-phenoxy-DL-phenylalanine amide hydrochloride (0.18 g), which was confirmed by an IR analysis, was obtained in the form of a white powder.

Provenance & Evidence