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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2351965Generated: November 1, 2026

Potassium Carbonate → HCID 14720281, compound

https://huagongshe.com/reaction/2351965

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant2-Propanesulfonyl chlorideHCID 82408—
Reactant4-chloro-N-(pyridin-3-ylmethyl)anilineHCID 2804545—
SolventChloroformHCID 6212—
ProductHCID 14720281HCID 14720281—

Reaction Steps

A 3.3 g. portion of 3-(4-chlorophenylaminomethyl)pyridine was dissolved in chloroform and reacted with 2.4 g. of isopropanesulfonyl chloride in the presence of 2.3 g. of potassium carbonate for several days at ambient temperature. The reaction mixture was worked up as described in Example 4, and the oily product was dissolved in chloroform and purified over silica gel, eluting with chloroform, to obtain 0.6 g. of the desired product, the elemental analysis which was as follows.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04874775
Source datasetuspto-grants-1989_10
ORD IDord-e1f8423e11bb4b69b7fdfca431db6319
Source noteuspto-grants-1989_10