HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14720281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | 4-chloro-N-(pyridin-3-ylmethyl)aniline | HCID 2804545 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14720281 | HCID 14720281 | — |
Reaction Steps
A 3.3 g. portion of 3-(4-chlorophenylaminomethyl)pyridine was dissolved in chloroform and reacted with 2.4 g. of isopropanesulfonyl chloride in the presence of 2.3 g. of potassium carbonate for several days at ambient temperature. The reaction mixture was worked up as described in Example 4, and the oily product was dissolved in chloroform and purified over silica gel, eluting with chloroform, to obtain 0.6 g. of the desired product, the elemental analysis which was as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04874775 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-e1f8423e11bb4b69b7fdfca431db6319 |
| Source note | uspto-grants-1989_10 |