HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54516331, compound → HCID 23353888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54516331 | HCID 54516331 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23353888 | HCID 23353888 | 98.8% |
Reaction Steps
To a solution of 3.89 g of methyl 4-(4-cinnamoylphenyl)butyrate in 50 ml of methanol, 0.25 g of 10% palladium on carbon was added, and hydrogenation was carried out at an ordinary temperature and under ordinary pressure for 5 hours. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give 3.87 g of pale brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597848 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-f810004691454dadb127cc60c74ba10a |
| Source note | uspto-grants-1997_01 |