4-Methoxybenzenesulfonyl chloride → 4-Methoxybenzenesulfonamide

HRID 2352063Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[OH-].[NH4+:14]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([NH2:14])(=[O:11])=[O:10])=[CH:5][CH:4]=1

Participants

Reactant 2

HCID 74014-Methoxybenzenesulfonyl chloride

HCID 14923Ammonium Hydroxide

Product 1

HCID 707894-Methoxybenzenesulfonamide

Procedure

Following the procedure described in Example 1, part B above, 94.94 g (0.45 m) of 4-methoxybenzenesulfonyl chloride from part A above was interacted with ammonium hydroxide to obtain 70.41 g of 4-methoxybenzenesulfonamide, shiny white crystals which melted at 111°-112° C.

Sources & evidence

ORD record: ord-1ed715bf7e784f34b7dfc2e58736ea0b
Source dataset: uspto-grants-1989_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04874894

Reaction notes

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