HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → 4-(Dodecyloxy)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 4-(Dodecyloxy)benzoic acid | HCID 75330 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-(Dodecyloxy)benzoyl chloride | HCID 12721043 | 103.4% |
Reaction Steps
4.0 g (1.31×10-2 mol) of p-dodecyloxybenzoic acid was dissolved in 15 ml of benzene, and 2.79 g (1.31×10-2 mol) of PCl5 was slowly added thereto under stirring at room temperature. Thereafter, 3 hours of heat-refluxing was effected, followed by distilling-off the solvent to obtain 4.4 g of p-dodecyloxybenzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876027 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-540154f32bf144f39b067a4630901bdc |
| Source note | uspto-grants-1989_10 |