HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanone, 1-nitro- → HCID 14230411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanone, 1-nitro- | HCID 66296 | — |
| Reactant | 3-Benzyloxybenzaldehyde | HCID 74342 | — |
| Reactant | HCID 70049071 | HCID 70049071 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 14230411 | HCID 14230411 | — |
Reaction Steps
10 mmol of 3-benzyloxybenzaldehyde and 10 mmol of 4-(6-oxo-1,4,5,6-tetrahydropyridazin-3-yl)benzyl 3-aminocrotonate are heated at 60° C. for 8 hours in 30 ml of i-propanol, a total of 20 mmol of nitroacetone being added in portions. The product crystallizes after addition of a little petroleum ether and trituration. It is recrystallized from a little i-propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04876254 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-1b1d20251cc347d8977b741e785c73b9 |
| Source note | uspto-grants-1989_10 |