HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 2-Dimethylaminopyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | CID 11268547 | HCID 11268547 | — |
| Reactant | HCID 15584310 | HCID 15584310 | — |
| Product | 2-Dimethylaminopyridine | HCID 21885 | — |
Reaction Steps
Following a procedure similar to that described in Example 1, but using 365 mg of radicicol, 11-cyanoundecanoyl chloride (prepared from 1.055 g of 11-cyanoundecanoic acid), 7 ml of dry methylene chloride, 1.21 ml of pyridine and a catalytic amount of dimethylaminopyridine, 707 mg of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597846 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-64bbf752fb15412e962e86a10c2ef4c1 |
| Source note | uspto-grants-1997_01 |