HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 235235Generated: October 25, 2026
Hexane → N-(2-Nitrophenyl)-N'-(3-bromo-4-ethoxyphenyl)-urea
https://huagongshe.com/reaction/235235
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 2-Nitrophenyl isocyanate | HCID 76834 | — |
| Reactant | 3-Bromo-4-ethoxyaniline | HCID 15270885 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(2-Nitrophenyl)-N'-(3-bromo-4-ethoxyphenyl)-urea | HCID 21473031 | — |
Reaction Steps
To a solution of 2-Nitrophenyl isocyanate (3.34 g) in 100 mL of toluene was added 3-Bromo-4-ethoxyaniline (3.1 g). The mixture was stirred at 20° C. for 30 min. Hexane (300 mL) was added and the resulting solid was filtered and dried to yield N-(2-Nitrophenyl)-N'-(3-bromo-4-ethoxyphenyl)-urea as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05597920 |
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| Source dataset | uspto-grants-1997_01 |
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| ORD ID | ord-c06e6e541095446bb7d71c417614983f |
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| Source note | uspto-grants-1997_01 |
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