HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl malonate → HCID 178516639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl malonate | HCID 7943 | — |
| Reactant | HCID 21473026 | HCID 21473026 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 178516639 | HCID 178516639 | — |
Reaction Steps
A mixture of 2-Fluoro-5-methoxybenzamidine (10.3 g) and dimethyl malonate (8.09 g) in dry dimethyl sulfoxide (7 mL) was allowed to stand at room temperature for 24 h.. The precipitated product was collected and washed with water and ether to afford 2-Phenyl-4,6-dihydroxy-pyrimidine as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05597920 |
| Source dataset | uspto-grants-1997_01 |
| ORD ID | ord-9ec5f1252a2241ac97785ae0a117a861 |
| Source note | uspto-grants-1997_01 |