HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Allyl-1-piperazinyl)-4-pentyloxyquinazoline → HCID 14424735, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Allyl-1-piperazinyl)-4-pentyloxyquinazoline | HCID 129560 | — |
| Reactant | Maleic Acid | HCID 444266 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14424735 | HCID 14424735 | 58.2% |
Reaction Steps
Ethanol (25 ml) was added to 2.3 g of maleic acid, and the mixture was heated to form a solution. A solution of 3.4 g of 2-(4-allyl-l-piperazinyl)-4-pentyloxyquinazoline in 5 ml of ethanol was added to the solution. The mixture was cooled, and the precipitated crystals were collected by filtration and recrystallized from 90 % ethanol to give 3.3 g of 2-(4-allyl-l-piperazinyl)-4-pentyloxyquinazoline dimaleate as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877790 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-556a1f48d6e746858402617f6ff93aa7 |
| Source note | uspto-grants-1989_10 |