HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 13773459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 5,8,11-Eicosatriynoic acid | HCID 1781 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13773459 | HCID 13773459 | — |
Reaction Steps
A solution of 8 g of 5,8,11-eicosatriynoic acid and 5.62 g of carbonyldiimidazole in 40 cm3 of anhydrous DMF is brought to 80° C. for 3 hours under an inert atmosphere. 3.25 g of ethanolamine are then added at 0° C. After 2 hours, it is verified by thin layer chromatography that the starting acid is completely converted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877789 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-63f35b0570484120befabf2548027892 |
| Source note | uspto-grants-1989_10 |