Ethanol → HCID 14071997, compound

HRID 2352561Notes

Reaction equation

HRID 2352561 reaction equation
C(OC([N:6]1[CH:18]=[C:17]([CH3:19])[C:16]2[C:8]([N:9]=[C:10]3[C:15]=2[C:14]([OH:20])=[CH:13][CH:12]=[CH:11]3)=[CH:7]1)=O)C.Br[C:22]1[CH:27]=[CH:26][C:25]([Cl:28])=[CH:24][N:23]=1.[CH3:29][CH2:30][OH:31].CN(C)[CH:34]=[O:35]>>[CH2:30]([O:31][C:34]([C:18]1[N:6]=[CH:7][C:8]2[NH:9][C:10]3[C:15]([C:16]=2[C:17]=1[CH3:19])=[C:14]([O:20][C:22]1[CH:27]=[CH:26][C:25]([Cl:28])=[CH:24][N:23]=1)[CH:13]=[CH:12][CH:11]=3)=[O:35])[CH3:29]

Participants

5

Reactant 4

HCID 702EthanolHCID 6228DimethylformamideHCID 8170982-Bromo-5-chloropyridineHCID 178473308HCID 178473308, compound

Product 1

HCID 14071997HCID 14071997, compound

Procedure

Analogously to Example 8 from 5-hydroxy-4-methyl-β-carboline-2-carboxylic acid ethyl ester and 2-bromo-5-chloropyridine in dimethylformamide, mp 194°-196° C. (EtOH).

Sources & evidence

ORD record
ord-404ae088aaa2442ea87325d2f223cf74
Source dataset
uspto-grants-1989_10
Patent number
US04877792

Reaction notes

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