Diisopropyl Ether → HCID 14071987, compound

HRID 2352564Notes

Reaction equation

HRID 2352564 reaction equation
[CH2:1]([C:3]1[N:7]=[C:6]([C:8]2[N:9]=[CH:10][C:11]3[NH:12][C:13]4[C:18]([C:19]=3[C:20]=2[CH2:21][O:22][CH3:23])=[C:17]([O:24][C:25]2[N:30]=[CH:29][CH:28]=CN=2)[CH:16]=[CH:15][CH:14]=4)[O:5][N:4]=1)[CH3:2].ClC1C=C[C:35](OC2C=CC=C3C=2C2C(COC)=C(C4ON=C(CC)N=4)N=CC=2N3)=[N:36]C=1.C(OC(C)C)(C)C>CCO>[CH2:1]([C:3]1[N:7]=[C:6]([C:8]2[N:9]=[CH:10][C:11]3[NH:12][C:13]4[C:18]([C:19]=3[C:20]=2[CH2:21][O:22][CH3:23])=[C:17]([O:24][C:25]2[CH:35]=[N:36][CH:28]=[CH:29][N:30]=2)[CH:16]=[CH:15][CH:14]=4)[O:5][N:4]=1)[CH3:2]

Participants

5

Reactant 3

HCID 7914Diisopropyl EtherHCID 14072005HCID 14072005, compoundHCID 14072006HCID 14072006, compound

Product 1

HCID 14071987HCID 14071987, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3-(3-ethyl-1,2,4-oxadiazol-5-yl)-4-methoxymethyl-5-(2-pyrimidinyloxy)-β-carboline, mp 175°-176° C. (EtOH), 5-(5-chloro-2-pyridyloxy)-4-methoxymethyl-3-(3-ethyl1,2,4-oxadiazol-5-yl)-β-carboline, mp 144°-146° C. (diisopropyl ether).

Sources & evidence

ORD record
ord-79f90ec54ea84b2091665ad154355e6e
Source dataset
uspto-grants-1989_10
Patent number
US04877792

Reaction notes

Loading…