HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 19843642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Thioglycerol | HCID 7291 | — |
| Reactant | 3,3-Dimethyl-1-butene | HCID 11210 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 19843642 | HCID 19843642 | — |
Reaction Steps
A mixture of 3-mercapto-1,2-propanediol (10.8 g), 3,3-dimethyl-1-butene (9.6 g) and 2,2'-azobis(2-methylpropionitrile) (0.5 g) is heated under reflux with vigorous stirring for 20 hours, then is diluted with hexane, extracted with water and stripped to give 3-(3,3-dimethylbutylthio)-1,2propanediol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877899 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-66b722dbf0fe41a4b544c989744b6fb4 |
| Source note | uspto-grants-1989_10 |