HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl hypochlorite → HCID 54172172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl hypochlorite | HCID 521297 | — |
| Reactant | ALLYL N-HEXYL SULFIDE | HCID 7010427 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54172172 | HCID 54172172 | — |
Reaction Steps
Tert-butyl hypochlorite (2.06 g, 19.0 mmol) is added dropwise at -50° to a solution of 3-hexylthio-1-propene (3.0 g, 19.0 mmol) in 20 ml of methylene chloride. The mixture is allowed to warm to RT and is then stripped of solvent to give 3-hexylthio-2-propenyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877899 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-a170d962d9b34614b4c37c38f98e250a |
| Source note | uspto-grants-1989_10 |