HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54335577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 54172172 | HCID 54172172 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 54335577 | HCID 54335577 | — |
Reaction Steps
3-Hexylthio-2-propenyl chloride is added to a solution of diisopropyl ethyl amine (3.68 g, 28.5 mmol) in 20 ml of methanol. The mixture is stirred overnight at RT. It is then diluted with hexane, washed with water and with brine and is stripped. The crude product is purified by prep. TLC to give 3-methoxy-1-hexylthio-1-propene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04877899 |
| Source dataset | uspto-grants-1989_10 |
| ORD ID | ord-3f5b6b6e640848808e565dc80061b09b |
| Source note | uspto-grants-1989_10 |