HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 131728238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | beta-Cyclodextrin | HCID 444041 | — |
| Reactant | HCID 15662541 | HCID 15662541 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 131728238 | HCID 131728238 | — |
Reaction Steps
2.5 grams of mequitazine in racemic or L- or D-form, 20.11 grams of β-cyclodextrin, and 5.11 grams of water are mixed and introduced into a 500 ml reactor. Carbon dioxide is then introduced into the reactor under a pressure of 15 MPa and at a temperature of 75° C. The unit is maintained under these operating conditions for 2 hours. The powder thus collected after releasing the medium is placed in a drying oven at 60° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07749982B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-9f2eafb09eb74f7b9aff34a4d60680c7 |
| Source note | uspto-grants-2010_07 |