HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 57418689, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 3-Bromo-6-chloroimidazo(1,2-b)pyridazine | HCID 12872323 | — |
| Product | HCID 57418689 | HCID 57418689 | 63.8% |
Reaction Steps
400 mg (1.72 mmol) of 3-bromo-6-chloroimidazo[1,2-b]pyridazine and 2.0 ml (33.4 mmol) of ethanolamine were stirred at 90° C. for 16 h. After cooling, the mixture was concentrated. The resulting residue was purified by chromatography (DCM/EtOH 9:1). 282 mg of the product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750000B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-94b7a938188c46c69e32877601ee37d4 |
| Source note | uspto-grants-2010_07 |