Butyric Acid → HCID 14800957, compound

HRID 2353204Notes

Reaction equation

[C:1](=[O:13])([S:11][CH3:12])[O:2][CH:3]([O:5][C:6](=[O:10])[CH:7]([CH3:9])C)C.Cl[C:15](OCCl)=O.C(O)(=O)CCC>>[C:1](=[O:13])([S:11][CH3:12])[O:2][CH2:3][O:5][C:6](=[O:10])[CH2:7][CH2:9][CH3:15]

Participants

Reactant 3

HCID 264Butyric Acid

HCID 62754Chloromethyl chloroformate

HCID 577926891-[[(Methylthio)carbonyl]oxy]ethyl 2-methylpropanoate

Product 1

HCID 14800957HCID 14800957, compound

Procedure

Following the procedures for synthesizing O-(1-isobutanoyloxyethyl) S-methyl thiocarbonate (2) and replacing 1-chloroethyl chloroformate with chloromethyl chloroformate in Step A and replacing isobutyric acid with n-butyric acid in Step B affords O-(butanoyloxymethyl) S-methyl thiocarbonate (8) as an oil.

Sources & evidence

ORD record: ord-77983d15de0f4e5a9247d66fb33bc5c4
Source dataset: uspto-grants-2010_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07749985B2

Reaction notes

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