Hydrochloric Acid → HCID 44818805, compound

Participants

Reaction Steps

The title compound (1.3 g, 95%) was prepared from the compound from step 1 (1.35 g, 3.8 mmol) and 4N HCl in dioxane by the procedure described in step 2 of Example 4: MS (ESI) m/z 381 (M+H); 1H NMR (400 MHz, DMSO-d6) δ 3.22 (br, 4H), 3.32 (t, J=5.6 Hz, 4H), 6.74 (d, J=8.8 Hz, 2H), 6.98-7.03 (m, 4H), 7.65 (d, J=8.8 Hz, 2H), 9.05 (br, 1H).

Provenance & Evidence