Sodium Hydroxide → HCID 58902530, compound

Participants

Reaction Steps

The title compound (15 mg. 38%) was prepared from the compound from step 1 (39 mg, 0.081 mmol) and 1N NaOH (0.11 mL, 0.11 mmol) by the procedure described in Example 2: MS (ESI) m/z 467 (M+1); 1H NMR (400 MHz, DMSO-d6) δ 1.59 (m, 2H), 1.83 (t, J=7.2 Hz, 2H), 2.27 (t, J=7.6 Hz, 2H), 2.47 (t, J=4.8 Hz, 4H), 3.09 (t, J=4.8 Hz, 4H), 6.74 (dd, J=2.0, 6.8 Hz, 2H), 6.91-6.98 (m, 4H), 7.63 (dd, J=2.4, 6.4 Hz, 2H).

Provenance & Evidence