Sodium Hydroxide → HCID 58902533, compound

Participants

Reaction Steps

The title compound (13 mg, 86%) was prepared from the compound from step 2 (15 mg, 0.035 mmol) and 1N NaOH (0.036 mL, 0.036 mmol) by the procedure described in Example 2: MS (ESI) m/z 409 (M+H). 1H NMR (400 MHz, CD3OD) δ 2.44 (m, 2H), 2.70 (t, J=4.8 Hz, 4H), 2.76 (m, 2H), 3.17 (t, J=4.8 Hz, 4H), 6.91-6.96 (m, 4H), 7.02 (m, 2H), 7.39 (dd, J=1.6, 4.8 Hz, 1H), 7.44 (m, 1H), 7.51 (dd, J=1.2, 2.8 Hz, 1H), 7.58 (m, 2H).

Provenance & Evidence