Methyl triflate → HCID 73446474, compound

Participants

Reaction Steps

To a suspension of 35 g (120 mmol) of phenyl(2-pyridyl)methanone O-benzyl oxime in 200 ml of diethyl ether are added dropwise, at 0° C., 17.4 ml (120 mmol) of methyl trifluoromethanesulfonate and the mixture is stirred at room temperature for 3 hours. The precipitate formed is collected by filtration and dried under reduced pressure.

Provenance & Evidence