Hydrochloric Acid → HCID 57931332, compound

Participants

Reaction Steps

To the product from Step A in 2 mL of methanol was added 2 mL of saturated hydrochloric acid in ethyl acetate. After stirring for 2 h the reaction was concentrated in vacuo and the residue purified by preparative thin layer chromatography using an Analtech® 1500 micron plate (20% methanol/ethyl acetate, 2% ammonium hydroxide) to give the title compound as a white solid. LC/MS 192.2 (M+1).

Provenance & Evidence