HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopropane → HCID 11689848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopropane | HCID 7840 | — |
| Reactant | 4-(Aminomethyl)-3-methoxyphenol | HCID 53404334 | — |
| Reactant | (1aS,5aR)-1,1,2-trimethyl-1,1a,5,5a-tetrahydro-3-thia-cyclopropa[a]pentalene-4-carboxylic acid | HCID 57892448 | — |
| Product | HCID 11689848 | HCID 11689848 | — |
Reaction Steps
(1aS,5aR)-1,1,2-Trimethyl-1,1a,5,5a-tetrahydro-3-thia-cyclopropa[a]pentalene-4-carboxylic acid 2-methoxy-4-propoxy-benzylamide is prepared starting from 4-aminomethyl-3-methoxy-phenol, bromopropane and (1aS,5aR)-1,1,2-trimethyl-1,1a,5,5a-tetrahydro-3-thia-cyclopropa[a]pentalene-4-carboxylic acid in analogy to the procedures given in Example 36. LC-MS: tR=1.13 min, [M+1]+=400.19.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750040B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-c48682f39aee40f1a7ab338911d59233 |
| Source note | uspto-grants-2010_07 |