HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-[Acetyl-(3,5-bistrifluoromethylbenzyl)amino]-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylic acid isopropyl ester → HCID 59003135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-[Acetyl-(3,5-bistrifluoromethylbenzyl)amino]-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylic acid isopropyl ester | HCID 11341306 | — |
| Reactant | Methyl 2-amino-3-(trifluoromethoxy)benzoate | HCID 53419547 | — |
| Product | HCID 59003135 | HCID 59003135 | — |
Reaction Steps
This compound was prepared utilizing the same methodology described in Example 1 wherein replacement of 2-amino-benzoic acid methyl ester with methyl 2-amino-3-trifluoromethoxybenzoate following the procedure of Example 1, Steps 1-8 for the synthesis of 5-[acetyl-(3,5-bistrifluoromethylbenzyl)amino]-2,3,4,5-tetrahydrobenzo[b]azepine-1-carboxylic acid isopropyl ester. CI MS 601 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07749992B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-aa27a0d7fca5408e9f82536d51b9a1a4 |
| Source note | uspto-grants-2010_07 |