HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dipentafluorophenylcarbonate → HCID 58816578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dipentafluorophenylcarbonate | HCID 2734833 | — |
| Reactant | HCID 55285766 | HCID 55285766 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58816578 | HCID 58816578 | — |
Reaction Steps
A solution of 2-ethyl-6-methyl-pyridin-4-ylamine (1.33 g, 9.8 mmol) in THF (25 mL) is slowly added to a solution of bis(pentafluorophenyl)carbonate (3.99 g, 10.1 mmol) in THF (10 mL). The mixture is stirred at r.t. for 48 h and the solution of title compound is used as stock solution for subsequent coupling reactions.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750161B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-622c78cf3993419b999429b8e85d2f9e |
| Source note | uspto-grants-2010_07 |