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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2354085Generated: October 30, 2026

HCID 11410496, compound → HCID 11248845, compound

https://huagongshe.com/reaction/2354085

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 11410496HCID 11410496—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 11248845HCID 11248845—

Reaction Steps

A suspension of 5-bromo-N-(1-{2-[3-(2,6-dimethyl-pyridin-4-yl)-ureido]-ethyl}-piperidin-4-yl)-N-ethyl-2-methoxy-benzenesulfonamide (Example 99, 30 mg, 0.05 mmol) and Pd—C (10%, 20 mg) in MeOH (10 mL) is stirred under hydrogen atmosphere for 15 h. The catalyst is filtered off and the reaction mixture evaporated to provide the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07750161B2
Source datasetuspto-grants-2010_07
ORD IDord-4ab2423d426042eaa2d8ba5b132cc760
Source noteuspto-grants-2010_07