HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-nitrobenzoic acid → N-[5-[(cyclopropylamino)carbonyl]-2-(trifluoromethyl)phenyl]-5-fluoro-2-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-nitrobenzoic acid | HCID 2737420 | — |
| Reactant | HCID 86049018 | HCID 86049018 | — |
| Product | N-[5-[(cyclopropylamino)carbonyl]-2-(trifluoromethyl)phenyl]-5-fluoro-2-nitrobenzamide | HCID 69565568 | — |
Reaction Steps
Using an analogous procedure to that described paragraph (A) in the portion of Example 1 which is concerned with the preparation of starting materials, 3-amino-N-cyclopropyl-4-(trifluoromethyl)benzamide was reacted with 5-fluoro-2-nitrobenzoic acid to give N-[5-[(cyclopropylamino)carbonyl]-2-(trifluoromethyl)phenyl]-5-fluoro-2-nitrobenzamide; Mass Spectrum: M−H+ 410.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07750154B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-69d2b87b62ea43829b384c931fe4f993 |
| Source note | uspto-grants-2010_07 |