Guanidine Hydrochloride → HCID 16045162, compound

HRID 2354923Notes

Reaction equation

HRID 2354923 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH:16]3[CH2:17][CH2:18][CH2:19][CH:12]2[C:13](=[CH:21]O)[C:14](=O)[CH2:15]3)(=[O:10])=[O:9])=[CH:4][CH:3]=1.Cl.[NH2:24][C:25]([NH2:27])=[NH:26]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:11]2[CH:16]3[CH2:17][CH2:18][CH2:19][CH:12]2[C:13]2[CH:21]=[N:24][C:25]([NH2:27])=[N:26][C:14]=2[CH2:15]3)(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 5742Guanidine HydrochlorideHCID 668419749-(4-Chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one

Product 1

HCID 16045162HCID 16045162, compound

Procedure

Prepared as described in Example 5 using 9-(4-chlorophenylsulfonyl)-2-(hydroxymethylene)-9-azabicyclo[3.3.1]nonan-3-one which was prepared as described in Example 34 and guanidine hydrochloride. See also: Hasan, Mashooda; Rashid, Naghmana; Khan, Khalid Mohammed; Snatzke, Guenther; Duddeck, Helmut; Voelter, Wolfgang Liebigs Annalen 1995, (5), 889-96.

Workup

  1. customPrepared
  2. customwas prepared

Sources & evidence

ORD record
ord-aaabf648b4da4d11874b9415bc94c67e
Source dataset
uspto-grants-2010_07
Patent number
US07754712B2

Reaction notes

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