HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → HCID 3378586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Product | HCID 3378586 | HCID 3378586 | 14.5% |
Reaction Steps
A mixture of ethyl acrylate (0.735 mol) and tert-butyl amine (0.210 mol) was refluxed for 6 days. The crude mixture was purified by fractionated distillation in vacuo (5 mbar). One fraction was collected (boiling point: 120° C. at 5 mbar), yielding to 8.3 g of the desired product as a light yellow oil. MS (m/e): 274.4 (MH+, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754736B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-547c085183ba4e469712cdce398c17bf |
| Source note | uspto-grants-2010_07 |