HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 86625823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 59383108 | HCID 59383108 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 86625823 | HCID 86625823 | — |
Reaction Steps
[2-(2,2-Difluoro-ethylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester (2.75 g, 10.9 mmol) was suspended in 4M hydrochloric acid in dioxane (30 ml) and stirred at RT for 18 h. Dichloromethane was added (50 ml) and the solid filtered off and dried in vacuo (2.02 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754746B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-150a3d916a3b4a4aa4e3256c6808b101 |
| Source note | uspto-grants-2010_07 |