HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 178446084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 58875107 | HCID 58875107 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178446084 | HCID 178446084 | — |
Reaction Steps
Hydroxylamine (600 μl) is added to a solution of N-(3-{(R)-2-[3-(5-cyano-indol-1-yl)-1,1-dimethyl-propylamino]-1-hydroxy-ethyl}-phenyl)-benzenesulphonamide (Example 1) (170 mg, 0.34 mmol) in 5 ml of ethanol. The reaction mixture is refluxed for 5 hours. Then the solvent is eliminated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754756B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-b83f26b9b60b43d8bd1779cea54f3105 |
| Source note | uspto-grants-2010_07 |