HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67192795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59382867 | HCID 59382867 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67192795 | HCID 67192795 | — |
Reaction Steps
tert-Butyl 3-((3-methoxypropoxy)(2-fluorophenyl)methyl)piperidine-1-carboxylate (28.0 mg, 0.07 mmol) was dissolved in 4 N HCl in dioxane. The resulting solution was stirred at rt until no starting material was left (˜30 min). The solvent was removed in vacuo to give 3-((3-methoxypropoxy)(2-fluorophenyl)methyl)piperidine hydrochloride as an oil. MS ESI+ve m/z 282 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754737B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-1a3700723ce44203b71e74aa43846613 |
| Source note | uspto-grants-2010_07 |