HRID2355345

反应详情

EQUATION

反应方程式

HRID 2355345 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

tert-Butyl 3-((3-methoxypropoxy)(2-fluorophenyl)methyl)piperidine-1-carboxylate (28.0 mg, 0.07 mmol) was dissolved in 4 N HCl in dioxane. The resulting solution was stirred at rt until no starting material was left (˜30 min). The solvent was removed in vacuo to give 3-((3-methoxypropoxy)(2-fluorophenyl)methyl)piperidine hydrochloride as an oil. MS ESI+ve m/z 282 (M+1).

WORKUP

后处理

  1. customThe solvent was removed in vacuo