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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2355830Generated: October 30, 2026

Ammonia → HCID 67543469, compound

https://huagongshe.com/reaction/2355830

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 67543089HCID 67543089—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 67543469HCID 6754346954%

Reaction Steps

2-{2-[3-(3-Piperidin-1-yl-propoxy)-phenyl-pyrrolidin-1-yl}-1-m-tolyl-ethanone. Prepared as described in Example 8, Step 1, on a 2.70 mmol scale, to give 610 mg (54%) of the desired product as an orange oil after chromatography (NH3 in MeOH/CH2Cl2). MS: exact mass calcd for C27H36N2O2, 420.3; m/z found, 421.5 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07754882B2
Source datasetuspto-grants-2010_07
ORD IDord-8107135f4d5445ad8f57255c726b6b0c
Source noteuspto-grants-2010_07