HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67543469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 67543089 | HCID 67543089 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 67543469 | HCID 67543469 | 54% |
Reaction Steps
2-{2-[3-(3-Piperidin-1-yl-propoxy)-phenyl-pyrrolidin-1-yl}-1-m-tolyl-ethanone. Prepared as described in Example 8, Step 1, on a 2.70 mmol scale, to give 610 mg (54%) of the desired product as an orange oil after chromatography (NH3 in MeOH/CH2Cl2). MS: exact mass calcd for C27H36N2O2, 420.3; m/z found, 421.5 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07754882B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-8107135f4d5445ad8f57255c726b6b0c |
| Source note | uspto-grants-2010_07 |