HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-(bromomethyl)-4-(trifluoromethyl)benzene → HCID 86633593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-(bromomethyl)-4-(trifluoromethyl)benzene | HCID 2756249 | — |
| Reactant | 4-(4,4-Dimethyl-2,5-dioxoimidazolidin-1-yl)-2-trifluoromethylbenzonitrile | HCID 11162285 | — |
| Product | HCID 86633593 | HCID 86633593 | 96% |
Reaction Steps
Compound 17.2 was prepared as described for example 6.2, by reacting compound 1.1 with 2-bromo-5-trifluoromethylbenzyl bromide. 4-[3-(2-Bromo-5-trifluoromethylbenzyl)-4,4-dimethyl-2,5-dioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile was obtained in a yield of 96%. (Molecular weight 533.01 (C21H14BrF6N3O2); retention time Rt=2.21 min. [B]; MS (ESI): 534.14 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759366B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-ac618e41e3c34592933214d3bce5c9f1 |
| Source note | uspto-grants-2010_07 |