HRID2356685

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID6371

Phosgene

CCl2O

HCID12186776

Tert-butyl 2-amino-2-methylpropanoate hydrochloride

C8H18ClNO2

HCID44158282

5-Amino[1,1′-biphenyl]-2-carbonitrile

C13H10N2

PRODUCTS

产物

反应SMILES：CC1(C)NC(=O)N(c2ccc(C#N)c(-c3ccccc3)c2)C1=O

HCID57829296

未命名化合物

PROCEDURE

实验过程

Compound 223.1 was prepared by the process as described for 1.1 by reaction of 223.3 with tert-butyl 2-amino-2-methylpropionate hydrochloride and phosgene (solution in toluene). 1H NMR: 8.73, s, 1H; 8.09, d, 1H, 7.75, s, 1H, 7.69, d, 1H, 7.62-7.5, m, 5H, 1.42, s, 6H.