HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → HCID 57829296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Tert-butyl 2-amino-2-methylpropanoate hydrochloride | HCID 12186776 | — |
| Reactant | 5-Aminobiphenyl-2-carbonitrile | HCID 44158282 | — |
| Product | HCID 57829296 | HCID 57829296 | — |
Reaction Steps
Compound 223.1 was prepared by the process as described for 1.1 by reaction of 223.3 with tert-butyl 2-amino-2-methylpropionate hydrochloride and phosgene (solution in toluene). 1H NMR: 8.73, s, 1H; 8.09, d, 1H, 7.75, s, 1H, 7.69, d, 1H, 7.62-7.5, m, 5H, 1.42, s, 6H.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759366B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-dbab09d5006d4350bff37c3cf64214ad |
| Source note | uspto-grants-2010_07 |