HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 67547197, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 54209632 | HCID 54209632 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67547197 | HCID 67547197 | — |
Reaction Steps
A mixture of methyl 6-methoxymethylnicotinate (737 mg) in a 2N aqueous sodium hydroxide solution (2 ml) and methanol (15 ml) was refluxed overnight. After cooling, the reaction mixture was concentrated under reduced pressure, and the resulting residue was triturated with diethyl ether to obtain 6-methoxymethylnicotinic acid sodium salt (754 mg) as colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759373B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-074b9f14a08146e58fbddb9ed063fd1d |
| Source note | uspto-grants-2010_07 |