HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → 2-Chloro-6-fluorobenzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 178505461 | HCID 178505461 | — |
| Product | 2-Chloro-6-fluorobenzothiazole | HCID 2049870 | — |
Reaction Steps
6-Fluoro-benzothiazole-2-thiol was treated with sulfuryl chloride by the procedure described in PCT/US04/14036 to give the desired product, which was used in the next step without further purification. EI-MS m/z 187 (M+); 1H NMR (DMSO-d6) δ 8.00 (m, 2H), 7.40 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759376B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-ec38302bd07d493e98a1b083e63ff14c |
| Source note | uspto-grants-2010_07 |