HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclopentane → HCID 22319193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclopentane | HCID 8728 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5'-Bromo[2,3'-bipyridin]-6'(1'H)-one | HCID 22319052 | — |
| Product | HCID 22319193 | HCID 22319193 | 19.9% |
Reaction Steps
2.00 g of 3-bromo-5-(2-pyridyl)-1,2-dihydropyridin-2-one as the stock material was N-alkylated by the normal method with 5.94 g of bromocyclopentane and 5.50 g of potassium carbonate, to obtain 506 mg of 3-bromo-1-cyclopentyl-5-(2-pyridyl)-1,2-dihydropyridin-2-one, 150 mg of which was treated in accordance with the method for Example 32, to obtain 120 mg of the subject compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759367B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-785875300f984d048ac97986b4a35959 |
| Source note | uspto-grants-2010_07 |