HCID 23110280, compound → HCID 23110289, compound

Participants

Reaction Steps

A mixture of 10.70 g 2-(2,2-diethoxy-ethoxy)-1-methoxy-4-nitro-benzene and 1.20 g of 10% palladium on carbon in 150 ml methanol was stirred for 2 hours under hydrogen atmosphere. The reaction mixture was filtered through a chem elut cartridge and the compound eluted with additional methanol. After contration under reduced pressure the residue was directly subjected to the subsequent reaction without further purification.

Provenance & Evidence