Iodoethane → HCID 59676114, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:13](=[CH:14][CH:15]=1)[NH:12][C:11]1[C:10]3[CH:16]=[CH:17][CH:18]=[CH:19][C:9]=3[S:8][CH2:7][C:6]2=1.[CH2:20](I)[CH3:21]>>[CH2:20]([N:12]1[C:11]2[C:10]3[CH:16]=[CH:17][CH:18]=[CH:19][C:9]=3[S:8][CH2:7][C:6]=2[C:5]2[C:13]1=[CH:14][CH:15]=[C:3]([O:2][CH3:1])[CH:4]=2)[CH3:21]Participants
3
Procedure
Following the procedure as in Example 33, using 8-methoxy-6,11-dihydro-5-thia-11-aza-benzo[a]fluorene (1.00 g, 3.75 mmol) and EtI (878 mg, 5.63 mmoL) as the starting material, the title compound was prepared as a white solid.
Sources & evidence
- ORD record
- ord-5a9b19f7d34147d3bb7fcc0e17f3f457
- Source dataset
- uspto-grants-2010_07
- Patent number
- US07759498B2
Reaction notes
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