HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 277395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | α-[(4-Hydroxy-3-methoxyphenyl)methylene]benzeneacetic acid | HCID 53411296 | — |
| Product | HCID 277395 | HCID 277395 | 88% |
Reaction Steps
A mixture of α-phenyl-4-hydroxy-3-methoxy cinnamic acid (0.0083 mol), NaHCO3 (10%, 5 mL), imidazole (2 mL) and polyethylene glycol (15 mL) were taken in a 250 mL iodine flask fitted with loose funnel at the top. The flask was shaken well and placed inside the microwave oven and irradiated (900 W) for 8 minutes in parts. After completion of reaction, the reaction mixture was worked (yield 88%) as in example I. Spectral data as given in example I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07759527B2 |
| Source dataset | uspto-grants-2010_07 |
| ORD ID | ord-1d020932b8c64380a0bfd91deba6906f |
| Source note | uspto-grants-2010_07 |