Sodium Bicarbonate → HCID 277395, compound

Participants

Reaction Steps

A mixture of α-phenyl-4-hydroxy-3-methoxy cinnamic acid (0.0083 mol), NaHCO3 (10%, 5 mL) methylimidazole (2 mL) and ethylene glycol (15 mL) were taken in a 250 mL round bottom flask fitted with reflux condenser. The flask was shaken well and placed on the heating mental and refluxed for 12 h. After completion of reaction, the reaction mixture was worked (yield 69%) as in example I. Spectral data as given in example I.

Provenance & Evidence